Sulfamic Acid: A Very Useful Catalyst

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Sulfamic acid: A green and efficient catalyst for synthesis of mono-, bis-, and spiro- perimidines

Mild and applicable synthesis of mono-, bis-, and spiro- perimidines is demonstrated in high yields via the condensation of 1,8-diaminonaphthalene and aldehydes or ketones in the presence of sulfamic acid as a green and highly efficient catalyst. This environmentally benign and clean synthetic pathway offers several advantages, such as high yields, short reaction times and easy work-up procedure.

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Silica-bonded n-propyldiethylenetriamine sulfamic acid as a recyclable solid acid catalyst for the synthesis of coumarin and biscoumarin derivatives

Silica-bonded n-propyldiethylenetriamine sulfamic acid (SBPDSA) was found as an efficient solid acid for the synthesis of coumarins. Coumarin derivatives were obtained via the Pechmann condensation reaction of phenols and β-keto-esters at 80 oC under solvent-free conditions. Also, biscoumarins were obtained via the condensation of aldehydes and 4-hydroxycoumarin in water at reflux conditions. T...

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Sulfamic acid: A green and efficient catalyst for synthesis of mono-, bis-, and spiro- perimidines

Mild and applicable synthesis of mono-, bis-, and spiro- perimidines is demonstrated in high yields via the condensation of 1,8-diaminonaphthalene and aldehydes or ketones in the presence of sulfamic acid as a green and highly efficient catalyst. This environmentally benign and clean synthetic pathway offers several advantages, such as high yields, short reaction times and easy work-up procedure.

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Silica-bonded n-propyldiethylenetriamine sulfamic acid as a recyclable solid acid catalyst for the synthesis of coumarin and biscoumarin derivatives

Silica-bonded n-propyldiethylenetriamine sulfamic acid (SBPDSA) was found as an efficient solid acid for the synthesis of coumarins. Coumarin derivatives were obtained via the Pechmann condensation reaction of phenols and β-keto-esters at 80 oC under solvent-free conditions. Also, biscoumarins were obtained via the condensation of aldehydes and 4-hydroxycoumarin in water at reflux conditions. T...

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Sulfamic acid supported on cellulose as a biodegradable and recyclable heterogeneous catalyst for the synthesis of tetrahydrobenzo xanthene derivatives

Cellulose bonded N-propyl diethylene tetra sulfamic acid (CBPDETSA) was successfully applied as a green and recyclable acidic catalyst for the synthesis of tetrahydrobenzo [a] xanthene-11-one as an important class of potentially bioactive compounds. The products are obtained by the coupling of 2-naphtol , cyclohexadione and aldehyde derivatives in good to high yields (70- 92%) under solvent-fre...

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ژورنال

عنوان ژورنال: Synlett

سال: 2005

ISSN: 0936-5214,1437-2096

DOI: 10.1055/s-2005-868479